Organic structure determination using 2-D NMR spectroscopy
a problem-based approach
Simpson, Jeffrey H.
creator
text
xxu
Amsterdam
Elsevier/AP
©2012
monographic
eng
xvi, 574 p. : illustrations ; 24 cm.
This book contains 30-40 quality 2D NMR data sets following an introductory section describing the methodology employed. Many other books describe the methods used, but none offer a large number of problems. Instructors at universities and colleges at the present time are forced to cobble together problems from a wide range of sources. The fragmentary approach to assembling course materials has a negative impact on course continuity and thus adversely impacts student retention. This book will stand as a single source to which instructors and students can go to obtain a comprehensive compe.
Chapter 1 - Introduction,
Chapter 2 - Instrumental Considerations,
Chapter 3 - Data Collection, Processing, and Plotting,
Chapter 4 - 1H and 13C Chemical Shifts,
Chapter 5 - Symmetry and Topicity,
Chapter 6 - Through-Bond Effects: Spin-Spin (J) Coupling,
Chapter 7 - Through-Space Effects: The Nuclear Overhauser Effect (NOE),
Chapter 8 - Molecular Dynamics,
Chapter 9 - Strategies for Assigning Resonances to Atoms within a Molecule,
Chapter 10 - Strategies for Elucidating Unknown Molecular Structures,
Chapter 11 - Simple Assignment Problems, Chapter 12 - Complex Assignment Problems,
Chapter 13 - Simple Unknown Problems,
Chapter 14 - Complex Unknown Problems,
Chapter 15 - More Assignment Problems,
Chapter 16 - More Unknown Problems,
Jeffrey H. Simpson.
Organic Structure
Data Collection
1H and 13C Chemical Shifts
Through-Bond Effects
Molecular Dynamics
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